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Beilstein J. Org. Chem. 2015, 11, 2646–2653, doi:10.3762/bjoc.11.284
Graphical Abstract
Figure 1: a) Schematic representation of the Aβ fibril formation. The monomeric peptide is shown as a colored...
Figure 2: a) Peptide boronic acids 1 and 2 are schematically shown as green sticks (peptide) with a red gripp...
Figure 3: Meso-erythritol is a promiscuous polyol which forms mixtures of esters due to the formation of 5-me...
Figure 4: Diol 5 (6.08 mg, 20.0 μmol, 1.0 equiv) and 3-(acetylamino)phenylboronic acid (6, 3.56 mg, 20.0 μmol...
Figure 5: Fmoc-Hot=Tap-OH (8).
Figure 6: Template 9 and boronic acid 6 can form the monoesters 10 and 11, or the diester 12. The signal assi...
Figure 7: Template 9 (2.30 mg, 4.40 µmol, 1.0 equiv) and peptide boronic acid 1 (7.35 mg, 8.80 µmol, 2.0 equi...
Figure 8: Template 5 (1H NMR expansion shown for reference DMSO-d6, 300 K) and peptide Leu-Val-Phe-Phe-Ala ar...
Figure 9: The trimeric template 16 together with 3 equivalents of pentapeptide LVFFA and 2-formylphenylboroni...